Jump to the main content block

Top

JEOL ECZ-600R 600MHz NMR

This instrument is a superconductor nuclear magnetic resonance spectrometer with a magnetic field strength of 14.09Tesla.It mainly tests liquid NMR spectra, including 1H, 13C, 15N, 31P, and nuclei with frequencies between 1H and 15N.The hydrogen resonance frequency is 600MHz, and it is capable of conducting variable temperature experiments and assisting in sample analysis.
Equipment Description

  • Brand and Model: JEOL ECZ600R, Japan
  • Standard magnetic field: 14.09 Tesla magnetic field and hydrogen resonance frequency of 600MHz
  • Main Accessories:
  1. Two probes:5mm Auto-Tune/Match Broadband Probe and 10mm Broadband Probe
  2. Variable Temperature Controller
  3. Computer workstation and NMR data processing software
  4. Auto Sample Changer

Service Items

  • One-dimensional homonuclear experiment: 1H spectrum, NOE effect, decoupling and reaction monitoring.
  • One-dimensional heteronuclear experiments: 13C, 15N, 19F, 27Al, 31P and other frequency spectra.
  • Two-dimensional experiments of biochemical molecules: COZY, NOESY, HSQC, HMBC, TOCSY, etc.
  • Measuring the structure and dynamic analysis of small molecules and macromolecules
  • Variable temperature experiment: isothermal or temperature gradient experiments in the temperature range of -100℃ to +100℃.

Charges

(a) Project reservation

  1. NT$130 for the first half hour, NT$80 for every half hour after
  2. NT$600 per sample for an overnight experiment (12-hour)
  3. 1D self-processing map NT$50 per half an hour
  4. In addition to the regular charges, variable temperature experiments are subject to an additional charge of NT$200 per unit.

(b) Non-project reservation

  1. NT$600 for the first half hour, NT$500 for every half hour after.
  2. NT$6000 per sample for an overnight experiment (12-hour).
  3. Substitute sample (not corrosive or odorous) fee is NT$200 per sample (test tube and solvent fee are not included)

Sample Preparation 

  • Samples must be prepared in 5 mm NMR tubes with a specification of 600 MHz or higher, and the height of the sample should be around 4 cm.
  • After preparing and handling the samples, please fill out the application form in detail, and make an online reservation. The service will be provided on a first-come, first-served basis.
  • Please make an appointment in advance for special services or unstable samples that are prone to decomposition.

Contact Detail
 

Instrument expert: Prof. Hsuan-Hung Liao
Technical staff: Chao-Lien Ho
contact method: (07)5252000 ext. 3989 nmr@mail.nsysu.edu.tw
Place: Chemistry Building 1F, Room CH1006
Click Num: